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In cells, LA is reduced to dihydrolipoic acid, which is generally regarded as the more bioactive form of LA and the form responsible for most of the antioxidant effects and for lowering the redox activities of unbound iron and copper

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After degassing the reaction mixture were added Pd 2 (dba) 3 (0.1 equiv.) and Xantphos (0.2 equiv.) and again degassed the reaction mixture for another 10 min